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Integration of a (13)C-(1)H satellite peak of a given (12)C-(1)H parent resonance within a quantitative (1)H NMR spectrum and comparison to the minor component represents a simple protocol for the accurate determination of diastereoisomeric ratios of up to 1000:1 (i.e., 99.8% de).

Original publication

DOI

10.1021/ol802211p

Type

Journal article

Journal

Org Lett

Publication Date

04/12/2008

Volume

10

Pages

5433 - 5436